Spark plasma sintering (SPS) is a highly efficient method for the preparation of a/β-SiAlON
ceramics. However, the rapid preparation of large-scale a/β-SiAlON ceramic components with
reliable mechanical properties is diffcult via SPS due to their near-insulating properties. In this
study, high-performance a/β-SiAlON ceramic end mill rods with large aspect ratios were
successfully prepared via SPS. Two different types of sintering processes (namely
vertical-round-rod (VRR) and horizontal-square-rod (HSR) processes) were developed, and their
effects on the phase composition, microstructure, mechanical properties, and machining
performance of the aB-SiAlON ceramic end mill rods were studied. The electric and temperature
field distributions during sintering were studied through an electro-thermal simulation. The
simulated and experimental temperature distributions are in good agreement. In contrast to VRR
samples, HSR samples with a small axial size show a uniform temperature distribution and
satisfactory microstructures within a certain range of dimensions as well as the expected phase
composition; furthermore, elongated B-SiAlON grains are preferentially oriented in the direction
perpendicular to the sintering pressure direction, As a result, the HSR samples exhibit better
mechanical properties and machining performance than the VRR samples.